Journal of Analytical Chemistry.
Vol. 59.
2004.
P. 163-167
Crystal and molecular structure of Bi-1,1′-(3,3-dimethyl-3,4- dihydroisoquinoline)
Bi-1,1′-(3,3-dimethyl-3,4-dihydroisoquinoline) (I) was synthesized. Its crystal structure was determined by X-ray diffraction analysis. Compound I crystallizes as isomer that is intermediate between the synand anti-forms with the angle of rotation between the bicyclic fragments equal to 90.1°. The N(1)=C(1) bond length is 1.276(4) ± 0.003 Å.
Authors
Sokol V.I.1
,
Glushkov V.A.2
,
Davydov V.V.
3
,
Sergienko V.S.
1
,
Merkur'eva N.Yu.
3
,
Shklyaev Yu.V.
2
Number of issue
2
Language
English
Pages
144-149
Status
Published
Link
Volume
30
Year
2004
Organizations
- 1 Kurnakov Inst. Gen. and Inorg. Chem., Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russian Federation
- 2 Institute of Technical Chemistry, Ural Division, Russian Academy of Sciences, ul Lenina 13, Perm, 614600, Russian Federation
- 3 Peoples' Friendship University, ul. Miklukho-Maklaya 6, Moscow, 117198, Russian Federation
Keywords
1,1' (3,3 dimethyl 3,4 dihydroisoquinoline); carbon; isoquinoline derivative; nitrogen; unclassified drug; article; chemical bond; chemical structure; crystal structure; crystallization; isomer; rotation; synthesis; X ray diffraction
Date of creation
19.10.2018
Date of change
14.04.2021
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Other records
Journal of Organic Chemistry.
Vol. 69.
2004.
P. 432-438