High-throughput small-molecule crystallography at the ‘Belok’ beamline of the Kurchatov synchrotron radiation source: Transition metal complexes with azomethine ligands as a case study

This paper concisely describes capabilities of the ‘Belok’ beamline at the Kurchatov synchrotron radiation source, related to high-throughput small-molecule X-ray crystallography. As case examples, a series of four novel transition metal complexes with azomethine ligands were selected. The complexes demonstrate somewhat unexpected changes in the coordination geometry and nuclearity in response to the introduction of substituents in the ligand’s periphery. © 2017 by the authors.

Авторы
Lazarenko V.A.1 , Dorovatovskii P.V.1 , Zubavichus Y.V.1 , Burlov A.S.2 , Koshchienko Y.V.2 , Vlasenko V.G.3 , Khrustalev V.N. 4
Редакторы
-
Журнал
Издательство
MDPI AG
Номер выпуска
11
Язык
Английский
Страницы
-
Статус
Опубликовано
Подразделение
-
Номер
325
Том
7
Год
2017
Организации
  • 1 National Research Center “Kurchatov Institute”, Moscow, 123182, Russian Federation
  • 2 Institute of Physical and Organic Chemistry, Southern Federal University, Rostov-on-Don, 344090, Russian Federation
  • 3 Institute of Physics of Southern Federal University, Rostov-on-Don, 344090, Russian Federation
  • 4 Peoples’ Friendship University of Russia (RUDN University), Moscow, 117198, Russian Federation
Ключевые слова
Azomethine ligands; Crystal structure; Kurchatov synchrotron radiation source; Secondary interactions; Transition metals
Дата создания
19.10.2018
Дата изменения
19.10.2018
Постоянная ссылка
https://repository.rudn.ru/ru/records/article/record/5224/