Synthesis, spectral characteristics, and the crystal and molecular structures of 2,3-dimethyl-1-phenyl-4-(N-phthalimido)pyrazolone-5

2,3-Dimethyl-1-phenyl-4-(N-phthalimido)pyrazolone-5 (I) is synthesized and isolated in the form of single crystals. The crystal structure of compound I is determined using X-ray diffraction. The phthalimide and pyrazolone rings in the molecule are not coplanar: the angle between their median planes is 56.4°. The bond lengths in the rings level off, which indicates the delocalization of the electron density. The spectral characteristics (IR and electronic spectra) of molecule I are determined. © 2008 Pleiades Publishing, Ltd.

Издательство
Springer
Номер выпуска
6
Язык
Английский
Страницы
998-1002
Статус
Опубликовано
Том
53
Год
2008
Организации
  • 1 Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskiǐpr. 31, Moscow 119991, Russian Federation
  • 2 Peoples' Friendship University of Russia, ul. Miklukho-Maklaya 6, Moscow 117198, Russian Federation
Ключевые слова
Crystal structure; Crystallography; Powders; Compound I; Crystal and molecular structures; Delocalization; Electron densities; IR and electronic spectrums; Phthalimide; Pyrazolone; Spectral characteristics; X-ray diffractions; Single crystals
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