Synthesis of 7-Bromo-1,3-diazapyrenes

An efficient synthetic route towards previously inaccessible 7-bromo-1,3-diazapyrenes through an in-melt peri-cyclization of readily available 7-(5-bromo-3,4-dihydropyrimidin-4-yl)-1H-perimidines is described. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim

Authors
Aksenov A.V. 1 , Shcherbakov S.V. 1 , Lobach I.V. 1 , Voskressensky L.G. 2 , Rubin M. 1, 3
Journal
European Journal of Organic Chemistry
Issue number
30
Language
English
Pages
4121-4127
State
Published
Link
External link
DOI
10.1002/EJOC.201800703
Volume
2018
Year
2018
Organizations
  • 1 Department of Chemistry, North Caucasus Federal University, 1a Pushkin St., Stavropol, 355009, Russian Federation
  • 2 Peoples' Friendship University of Russia, 6 Miklukho-Maklaya St., Moscow, 117198, Russian Federation
  • 3 Department of Chemistry, University of Kansas, 1251 Wescoe Hall Dr., Lawrence, KS 66045-7582, United States
Keywords
Annulation; Nitrogen heterocycles; Polycycles; Synthetic methods; Thermolysis
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