New Method for the Synthesis of 1-Substituted (3a,6a)-Diaryl­glycolurils

A new approach has been developed for the synthesis of 1-substituted 3а,6а-diarylglycolurils from an imidazolone, imidazo­oxazolone, imidazooxazinone, or imidazooxazepinone and urea in the presence of hydrochloric acid. The structure of 1-ethyl-3а,6а-diphenylglycoluril was confirmed by X-ray diffraction studies. © Georg Thieme VerlagStuttgart · New York.

Authors
Baranov V.V. 1, 2 , Antonova M.M. 1 , Nelyubina Y.V. 3 , Kolotyrkina N.G. 1 , Kravchenko A.N. 1
Journal
Issue number
6
Language
English
Pages
669-672
State
Published
Number
st-2016-d0733-l
Volume
28
Year
2017
Organizations
  • 1 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., Moscow, 119991, Russian Federation
  • 2 Рeoples’ Friendship University of Russia, 6 Miklukho-Maklaya St., Moscow, 117198, Russian Federation
  • 3 A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 Vavilova St., Moscow, 119991, Russian Federation
Keywords
condensation; glycolurils; imidazolones; polycycles; urea
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