Unexpected Formation of [(∆ 3-Piperideino)pyrimidino]-14-crown-4 Ethers in a Petrenko-Kritschenko Type Condensation

Two novel aza-14-crown-4 ether derivatives bearing fused (∆ 3 -piperideino)[2,3-e]pyrimidine moieties as subunits were unexpectedly obtained as major products of a modified Petrenko-Kritschenko type cascade condensation of 1-benzyl-4-ethoxycarbonylpiperidin-3-one with 1,5-bis(2-formylphenoxy)-3-oxapentane and ammonium acetate. X-ray structure study was performed to determine the structure of the compounds.

Authors
Hieu T.H. 1 , Anh L.T. 1 , Soldatenkov A.T. 2 , Vasil'ev V.G. 2 , Kotsuba V.E. 2 , Khrustalev V.N. 3
Journal
Macroheterocycles
Issue number
4
Language
English
Pages
379-382
State
Published
Volume
6
Year
2013
Organizations
  • 1 Vietnam National University
  • 2 Peoples’ Friendship University of Russia
  • 3 Nesmeyanov Institute of Organoelement Compounds
Keywords
Aza-14-crown-4 ether; multicomponent reaction; Petrenko-Kritschenko condensation; X-ray structure
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