Two-dimensional NMR spectra of 17α-(1-aziridinylmethyl)-5α-androstan-17β-ol

The complex1H and13C NMR spectra of 17α-(1-aziridinylmethyl)-5α-androstan-17β-ol were analyzed using two-dimensional (2M) spectroscopy. The configuration of the substituents at the 17 position was determined using the 2M-spectroscopy of the nuclear Overhauser effect. The direct13C-13C SSCCs were determined. © 1989 Plenum Publishing Corporation.

Authors
Aliev A.E. 1, 2, 3 , Fomichev A.A. 1, 2, 3 , Sova A.N. 1, 2, 3 , Gella I.M. 1, 2, 3 , Kostyanovskii R.G. 1, 2, 3
Journal
Chemistry of Heterocyclic Compounds
Publisher
Латвийский институт органического синтеза Латвийской академии наук / Springer New York Consultants Bureau
Number of issue
11
Language
English
Pages
1212-1216
Status
Published
Link
External link
DOI
10.1007/BF00633497
Volume
24
Year
1988
Organizations
  • 1 P. Lumumba Peoples' Friendship University, Moscow, 117923, Russian Federation
  • 2 Khar'kov Scientific Research Institute of the Endocrinology and Chemistry of Hormones, Khar'kov, 310002, Ukraine
  • 3 Institute of Chemical Physics, Academy of Sciencies of the USSR, Moscow, 117977, Russian Federation
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DEHYDRATION OF 10,10-DIMETHYL-9-ALLYL-9,10-DIHYDRO-10-SILA-2-AZAANTHROL-9

Article
Prostakov N.S., Varlamov A.V., Kozm K., Fomichev A.A., Aliev A.E., Pal'ma A., Kandzhi P.
Chemistry of Heterocyclic Compounds. Латвийский институт органического синтеза Латвийской академии наук / Springer New York Consultants Bureau. Vol. 24. 1988. P. 1303-1306