Russian Chemical Bulletin.
Vol. 71.
2022.
P. 819-823
Homocondensation of acetylferrocene under ultrasonic conditions
The cyclocondensation of 1-acetylferrocene was studied in the presence of p-toluenesulfonic acid under ultrasonic conditions at 80 °C. The reaction was found to produce ethyl ferrocenoate along with 1,3,5-triferrocenylbenzene and 1,3-diferrocenylbenzene. The structure of ethyl ferrocenoate was studied by NMR spectroscopy and X-ray diffraction. © 2022, Springer Science+Business Media LLC.
Authors
Dvorikova R.A.1
,
Dorovatovski P.V.2
,
Mitrophanova A.V.
3
,
Khrustalev V.N.
3,
4
,
Kovalev A.I.1
Journal
Number of issue
4
Language
English
Pages
717-721
Status
Published
Link
Volume
71
Year
2022
Organizations
- 1 A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, Moscow, 119991, Russian Federation
- 2 National Research Center “Kurchatov Institute”, 1 ul. Akad. Kurchatova, Moscow, 123182, Russian Federation
- 3 Peoples’ Friendship University of Russia (RUDN University), 6 ul. Miklukho-Maklaya, Moscow, 117198, Russian Federation
- 4 N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., Moscow, 119991, Russian Federation
Keywords
1,3,5-triferrocenylbenzene; 1,3-diferrocenylbenzene; acetylferrocene; ethyl ferrocenoate; sonochemistry; trimerization cyclocondensation; X-ray diffraction
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