Reaction of 1-hydrazino-3,3-dimethyl-3,4-dihydroisoquinoline with ethyl acetoacetate. The crystal structure and IR spectra of ethyl 3-(3,3-dimethyl-1,2,3,4-tetrahydroisoquinolylidenehydrazono)-2-oxobutanoate

The reaction of 1-hydrazino-3,3-dimethyl-3,4-dihydroisoquinoline with ethyl aceto-acetate afforded ethyl 3-(3,3-dimethyl-1,2,3,4-tetrahydroisoquinolylidenehydrazono)-2-oxobutanoate. The crystal structure of the title compound was established by X-ray diffraction analysis.

Authors
Sokol V.I.1 , Davydov V.V. 2 , Shklyaev Yu.V.3 , Glushkov V.A.3 , Sergienko V.S.1
Journal
Russian Chemical Bulletin
Number of issue
5
Language
English
Pages
957-961
Status
Published
Link
External link
DOI
10.1007/BF02494644
Volume
48
Year
1999
Organizations
  • 1 N. S. Kurnakov Inst. of Gen. and I., Russian Academy of Sciences, 31 Leninsky prosp., 117907 Moscow, Russian Federation
  • 2 Russian Friendship University, 6 ul. Miklukho-Maklaya, 117198 Moscow, Russian Federation
  • 3 Institute of Technical Chemistry, Ural Br. of the Russ. Acad. of Sci., 116 ul. Bol'shevistskaya, 614000 Perm', Russian Federation
Keywords
1-hydrazino-3,3-dimethyl-3,4-dihydroisoquinoline; Crystal structure; Ethyl 3-(3,3-dimethyl-1,2,3,4-tetrahydroisoquinolylidenehydrazono)-2-oxobutanoate; IR spectra
Date of creation
19.10.2018
Date of change
16.04.2021
Short link
https://repository.rudn.ru/en/records/article/record/611/
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