Spectral and thermochemical properties of the [Na(H 2O) 4] [EuL 4]·0.775CH 2Cl 2 complex, HL = 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione

Reaction of Eu(NO 3) 3·6H 2O with 1,3-bis(1,3-dimethyl-1H-pyrazol-4-yl)-1,3-propanedione (HL) in the presence of NaOH affords the complex compound [Na(H 2O) 4] [EuL 4]·0.775CH 2Cl 2 (I). The spectral (UV, IR, 1H NMR spectroscopy), and thermo-luminescent (TG-DSC-MS) properties of the complex I, as well as its fragmentation at the laser desorption ionization (LDI-MS) were studied. © Pleiades Publishing, Ltd., 2011.

Authors
Taidakov I.V. 1 , Zaitsev B.E. 2 , Krasnosel'skii S.S. 2 , Borisov R.S. 3
Journal
Russian Journal of General Chemistry
Number of issue
10
Language
English
Pages
2176-2182
Status
Published
Link
External link
DOI
10.1134/S1070363211100239
Volume
81
Year
2011
Organizations
  • 1 Petrov Institute of Plastics, Perovskii proezd 35, Moscow, 111024, Russian Federation
  • 2 Russian Peoples' Friendship University, ul. Mikluho-Maklaya 6, Moscow, 117198, Russian Federation
  • 3 Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russian Federation
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