Physics of Atomic Nuclei.
Vol. 75.
2012.
P. 525-529
Assessing the capabilities of direct analysis in real time mass spectrometry for 5-hydroxymethylfurfural quantitation in honey
The limitations of direct analysis in real time mass spectrometry (DART-MS) were shown with the example of 5-hydroxymethylfurfural (HMF) quantitation in honey. An accurate analyte quantitation was impossible because the carbohydrate matrix partially degraded to the analyte in the ionization region. However, at a decreased DART temperature of 150 °C, the DART-MS screening was possible using two spiked reference samples. The influence of instrumental parameters on the composition of the DART mass spectra for HMF and carbohydrates was investigated. Also, first data on scanning surface analysis with DART-MS were obtained giving rise for further studies in this direction. © 2012 Elsevier B.V. All rights reserved.
Authors
Chernetsova E.S.
1,
3
,
Morlock G.E.1,
2
Language
English
Pages
22-32
Status
Published
Link
Volume
314
Year
2012
Organizations
- 1 Institute of Food Chemistry, University of Hohenheim, Garbenstrasse 28, 70599 Stuttgart, Germany
- 2 Institute of Nutritional Science, Justus-Liebig-University of Gießen, Heinrich-Buff-Ring 26, 35392 Gießen, Germany
- 3 People's Friendship University of Russia, Miklukho-Maklaya St. 6, 117198 Moscow, Russian Federation
Keywords
5- Hydroxymethylfurfural; Carbohydrates; Direct analysis in real time mass spectrometry; HMF; Honey; Screening
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