Compactability Regularities Observed during Cold Uniaxial Pressing of Layered Powder Green Samples Based on Ti-Al-Nb-Mo-B and Ti-B

We determined the compactability regularities observed during the cold uniaxial pressing of layered powder green samples, taking into account factors such as composition, height, and number of Ti–B (TiB) and Ti–Al–Nb–Mo–B (TNM) layers. The following composition was chosen for the TNM layer at %: 51.85Ti–43Al–4Nb–1Mo–0.15B, while for the Ti-B layer we selected the composition wt %: Ti-B-(20, 30, 40) Ti. Green samples were made containing both 100 vol % TiB and TNM, and those taken in the following proportions, vol %: 70TiB/30TNM, 50TiB/50TNM, 30TiB/70TNM; multilayer green samples were studied in the following proportions, vol %: 35TiB/30TNM/35TiB, 25TiB/25TNM/25TiB/25TNM, 35TNM/30TiB/35TNM. Based on the obtained rheological data, we determined the rheological characteristics of the layered green samples, including compressibility modulus, compressibility coefficient, relaxation time, and limiting value of linear section deformation. These characteristics were found to vary depending on the composition, height, and number of layers. Our findings revealed that reducing the TNM content in the charge billet composition improves the compaction of powder materials under the given technological parameters of uniaxial cold pressing. Moreover, we observed that increasing the boron content and decreasing the amount of titanium in the Ti–B composition enhances the compactability of powder materials. We also established a relationship between the compaction pressure interval and the density of the layered powder green sample. © 2023 by the authors.

Authors
Bazhin P. , Konstantinov A. , Chizhikov A. , Antipov M. , Stolin P. , Avdeeva V. , Antonenkova A.
Journal
Publisher
MDPI AG
Number of issue
11
Language
English
Status
Published
Number
1827
Volume
13
Year
2023
Organizations
  • 1 Merzhanov Institute of Structural Macrokinetics and Materials Sciences, Russian Academy of Sciences, ul. Akademika Osipyana 8, Chernogolovka, 142432, Russian Federation
  • 2 Department “Nanotechnology and Microsystem Technology, RUDN University, Miklukho-Maklaya Str. 6, Moscow, 117198, Russian Federation
  • 3 Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii Prospekt 31, Moscow, 119991, Russian Federation
Keywords
cold uniaxial pressing; compactability; layered composite materials; powder green samples; rheological regularities; titanium boride; TNM
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